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Equipment

The pH meter and its calibration

Do I need a pH meter for cider, and how do I keep it accurate?

In short

A pH meter consists of a glass electrode that develops a small voltage proportional to hydrogen ion activity, a reference electrode, and a meter that converts that voltage into a pH reading.

pH matters in cider for two reasons that have nothing to do with taste. It determines which spoilage organisms can grow, and it determines what fraction of any added sulphur dioxide exists in the molecular form that actually does the antimicrobial work.

The instrument is only as good as its last calibration. An uncalibrated meter gives a confident number that may be wrong by enough to change a decision entirely.

Why pH and not acidity

Total acidity and pH measure different things and are not interchangeable. Total acidity is how much acid is present in total, found by titration; pH is how acidic the solution behaves, which depends on how much of that acid has dissociated and on what else in the liquid is buffering it. Two ciders with identical total acidity can differ in pH by a wide margin, most often because of differences in potassium content, which comes from the fruit and the soil.

The palate responds mostly to total acidity. Microbiology and sulphite chemistry respond to pH. That is why a maker who wants to know how a cider will taste titrates, and a maker who wants to know whether it is safe measures pH — and why both instruments earn their place.

The pH also sets the antimicrobial value of sulphur dioxide. Only the molecular form is effective, and the proportion in that form falls sharply as pH rises, so the same addition that protects a low-pH juice may do very little in a high-pH one. Any dosing decision made without a pH reading is being made blind, which is why CiderHQ points readers at the supplier’s own dosing guidance in conjunction with a measured pH rather than at a remembered figure.

Calibrating properly

Calibration is done against standard buffer solutions of known pH, at the temperature the samples will be at. Two-point calibration, typically with a pH 7.00 buffer and a pH 4.00 buffer, brackets the range cider sits in and corrects both the offset and the slope of the electrode response. A single-point calibration corrects the offset only and is not adequate for a working instrument.

Buffers have a shelf life and are contaminated by the probe itself. They are poured into a small clean vessel for use and discarded afterwards, never returned to the bottle. A bottle of buffer that has been dipped into repeatedly for a season is not a standard any more.

Frequency depends on use and on how much the decision depends on the number. Calibrating at the start of every session in which pH will be used for a decision is the defensible practice; calibrating once a year is not. A meter whose slope has degraded beyond the range the instrument will accept is telling you the probe has reached the end of its life.

Looking after the probe

Temperature and reading discipline

pH varies with temperature, and a meter with automatic temperature compensation corrects the electrode’s response but not the genuine temperature dependence of the sample itself. Readings are therefore taken at a consistent temperature, and a pH quoted without a temperature is incomplete for any careful purpose.

A reading is taken with the probe stirred gently in the sample and allowed to stabilise, which may take a minute or more on a cold sample or an ageing probe. Recording a number the moment it appears on the screen is the commonest source of avoidable error.

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