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Titration kits for total acidity

How do I measure the acidity of cider?

In short

A known volume of degassed cider or juice is placed in a flask and a standard sodium hydroxide solution is added from a burette or syringe until the acid is exactly neutralised. The volume of alkali used is proportional to the acid present.

In cider the result is conventionally expressed as grams per litre of malic acid, because malic is the dominant acid in apples. Wine convention uses tartaric acid instead, so a figure quoted without saying which acid it is expressed as is ambiguous and can differ by a noticeable factor.

This is the number that predicts how sharp a cider tastes, and the number a blender works with. It is distinct from pH and neither substitutes for the other.

How the measurement works

Titration exploits a simple stoichiometry: alkali neutralises acid mole for mole of available hydrogen ion. If the concentration of the alkali is known exactly, then the volume needed to reach neutralisation gives the amount of acid in the sample directly. The arithmetic that converts that volume into grams per litre of malic acid depends on the alkali concentration, the sample volume and the equivalent weight of the acid it is being expressed as.

The endpoint in wine and cider work is conventionally taken at pH 8.2 rather than at pH 7, because the weak organic acids involved are not fully neutralised at 7. That convention is what makes results comparable between laboratories, and it is why a titration followed with a pH meter is set to stop at 8.2.

The sample must be degassed first. Dissolved carbon dioxide is itself an acid and will be titrated along with everything else, inflating the result. Degassing is done by warming, by vigorous stirring, or under vacuum, depending on the kit.

The endpoint problem

Simple kits use phenolphthalein, an indicator that turns from colourless to pink around the right pH. In white wine or pale juice this works well. In a deeply coloured traditional cider — brown, orange or amber from oxidised phenolics — the colour change is masked and the endpoint is a matter of guesswork, which is the commonest reason a home titration disagrees with a laboratory.

There are two practical answers. The first is to dilute the sample heavily with distilled water before titrating: dilution does not change the amount of acid present, so it does not change the result, but it makes the colour change visible. The second, and better, is to titrate to a pH meter reading of 8.2 and ignore the indicator entirely, which removes the judgement from the process.

Kits sold for home use vary considerably in quality. What determines accuracy is the accuracy of the sample measurement, the accuracy of the alkali concentration, and the resolution of whatever delivers the alkali. A syringe graduated in half millilitres is a coarser instrument than a burette, and on a small sample that coarseness dominates the result.

Reagents and their limits

Sodium hydroxide solution absorbs carbon dioxide from the air and weakens over time, so its concentration drifts. Kits supply it in sealed containers with a shelf life for that reason, and a bottle that has been open on a shelf for two seasons will give results that read low. Where the number matters, the alkali is standardised against a known acid before use, or replaced.

Sodium hydroxide is caustic, and even the dilute solutions used in titration kits will damage eyes. Eye protection is worn, the supplier’s safety data sheet governs handling and disposal, and it is stored where it cannot be mistaken for anything else.

The instruments — pipette, flask, burette — are rinsed with distilled water and then with a little of the solution they will hold, so that residual water does not dilute what is being measured.

What the number is used for

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